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The Samples Were Homogenized In A Ball Mill

Samples were homogenized in a ball mill 20 hz, 5 min, 22c, mm 400, rentsch, haan, germany.The crude suspension was then hydrolysed for 30 min at 60c.Directly after hydrolysis, samples were neutralized ph 6-7 on ice with 70 l of 50 acetic acid and extracted as described below.Lipid extraction.

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